2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

Base Information

Chemical Name:2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide
CAS No.:1092446-08-6
Molecular Formula:C₂₄H₂₃F₃N₂O₄S
Molecular Weight:492.519
Hs Code.:

Synonyms:2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

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Chemical Property of 2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

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Technology Process of 2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

There total 5 articles about 2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 421-85-2
Trifluoromethanesulfonamide

: 1092445-60-7
2-(2-cyclopent-1-enyl-3-methyl-benzoylamino)-indan-2-carboxylic acid

: 1092446-08-6
2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 80h;

Reference yield:

: 1092447-82-9
2-(2-iodo-3-methyl-benzoylamino)-indane-2-carboxylic acid ethyl ester

: 1092446-08-6
2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 2.7 h / 110 °C / Microwave irradiation

2.1: potassium hydroxide; ethanol; water / 8 h / 20 °C

2.2: pH ~ 3

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 80 h

With dmap; potassium hydroxide; ethanol; water; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: 91-13-4
α,α'-dibromo-o-xylene

: 1092446-08-6
2-cyclopent-1-enyl-3-methyl-N-(2-trifluoromethanesulfonylaminocarbonyl-indan-2-yl)-benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / acetonitrile / 75 °C

2.1: hydrogenchloride; water / ethanol / 5 h / 20 °C

2.2: pH 10

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.08 h

3.2: 118 h

4.1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 2.7 h / 110 °C / Microwave irradiation

5.1: potassium hydroxide; ethanol; water / 8 h / 20 °C

5.2: pH ~ 3

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 80 h

With hydrogenchloride; dmap; potassium hydroxide; ethanol; water; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; dichloromethane; water; acetonitrile;