3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

Base Information

Chemical Name:3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide
CAS No.:1415135-19-1
Molecular Formula:C₁₈H₁₈BrN₃O₃S₂
Molecular Weight:468.395
Hs Code.:

Synonyms:3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

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Chemical Property of 3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

Chemical Property:

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Technology Process of 3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

There total 6 articles about 3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1377582-43-8
4-isopropoxy-3-thioureido-benzenesulfonamide

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 1415135-19-1
3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

Guidance literature:: 4-isopropoxy-3-thioureido-benzenesulfonamide; para-bromophenacyl bromide; In ethanol; at 75 ℃; for 3h;

With sodium hydrogencarbonate; In water; for 1.5h;

Reference yield:

: 406233-31-6
4-fluoro-3-nitrobenzenesulfonamide

: 1415135-19-1
3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium / 2.5 h / Reflux

1.2: 3.67 h / 20 °C

2.1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 0.5 h / 0 - 23 °C

3.1: sodium hydrogencarbonate / chloroform; water / 1.5 h / 20 °C

4.1: ammonia / methanol / 18 h / 20 °C

5.1: ethanol / 3 h / 75 °C

5.2: 1.5 h

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; ammonia; sodium; sodium hydrogencarbonate; In methanol; ethanol; chloroform; water;

Reference yield:

: 90566-23-7
3-Amino-4-isopropoxy-benzenesulfonamide

: 1415135-19-1
3-((4-(4-bromophenyl)thiazol-2-yl)amino)-4-isopropoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / chloroform; water / 1.5 h / 20 °C

2.1: ammonia / methanol / 18 h / 20 °C

3.1: ethanol / 3 h / 75 °C

3.2: 1.5 h

With ammonia; sodium hydrogencarbonate; In methanol; ethanol; chloroform; water;