(1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

Base Information

Chemical Name:(1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol
CAS No.:464892-38-4
Molecular Formula:C₁₅H₂₈O₂
Molecular Weight:240.386
Hs Code.:

Synonyms:(1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

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Technology Process of (1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

There total 2 articles about (1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 103615-39-0
(1R,2R,5R)-5-methyl-2-((S)-2-methyloxiran-2-yl)cyclohexanol

: 503-60-6
3,3-dimethyl-allyl chloride

: 464892-38-4
(1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

Guidance literature:: With copper(l) iodide; magnesium; In tetrahydrofuran; dichloromethane; at -30 ℃; for 1.5h;
DOI:10.1016/S0040-4039(02)00939-5

Reference yield:

: 7786-67-6,18674-65-2,20549-46-6,21290-09-5,29141-10-4,50373-36-9,59905-53-2,59905-54-3,96612-21-4,104870-56-6,121468-66-4,122517-60-6,122517-61-7,144541-38-8,89-79-2
isopulegol

: 464892-38-4
(1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 48.2 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 3 h / 0 °C

2.1: Mg; 1,2-dichloroethane / tetrahydrofuran

2.2: 95 percent / copper(I) iodide / tetrahydrofuran / 1.5 h / -30 °C

With magnesium; 1,2-dichloro-ethane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(03)01168-2

Reference yield: 75.0%

: 464892-38-4
(1R,2R,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanol

: 464892-40-8
(2S,5R,1'S)-2-(1'-hydroxy-1',5'-dimethyl-4'-hexenyl)-5-methylcyclohexanone

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1016/S0040-4039(02)00939-5