C₅₄H₆₈N₄O₁₀

Base Information

Chemical Name:C₅₄H₆₈N₄O₁₀
CAS No.:362516-95-8
Molecular Formula:C₅₄H₆₈N₄O₁₀
Molecular Weight:933.155
Hs Code.:

C<sub>54</sub>H<sub>68</sub>N<sub>4</sub>O<sub>10</sub>

Synonyms:C₅₄H₆₈N₄O₁₀

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Chemical Property of C₅₄H₆₈N₄O₁₀

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Technology Process of C₅₄H₆₈N₄O₁₀

There total 16 articles about C₅₄H₆₈N₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 362517-11-1
(3aR,4S,5S,11bS)-methyl 2,3,3a,4,5,7-hexahydro-4-[(2S)-2-ethyl-2,3-(isopropylidenedioxy)propyl]-1H-pyrrolo[2,3-d]carbazole-5-hydroxymethyl-6-carboxylate

: 362516-95-8
C₅₄H₆₈N₄O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

2.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

2.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

3.1: thiocresol / 2 h / 110 °C

3.2: tributyltin hydride; 2,2'-diazobisisobutyronitrile / toluene / 24 h / Heating

3.3: H₂; triethylamine / Pd(OH)2/C / ethyl acetate / 1 h

4.1: 1.231 g / triethylamine; potassium carbonate / acetone / 15 h

5.1: tert-butyl hypochlorite; triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

6.1: tetrafluoroboric acid-dimethyl ether copmlex; silver tetrafluoroborate / acetone / 1 h / -10 °C

7.1: 4.2 percent / KBH₄ / acetic acid / 0.5 h / 0 °C

8.1: 0.045 g / aq. hydrochloric acid / methanol

With hydrogenchloride; dmap; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; p-toluenesulfonylanhydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; para-thiocresol; tetrafluoroboric acid dimethyl ether complex; In methanol; dichloromethane; water; acetic acid; acetone;
DOI:10.1021/jo000250y

Reference yield:

: 362517-06-4
(3aR,4S,5S,11bS)-dimethyl 3-benzyl-2,3,3a,4,5,7-hexahydro-4-[(2R)-2-ethyl-2,3-epoxypropyl]-1H-pyrrolo[2,3-d]carbazole-5,6-dicarboxylate

: 362516-95-8
C₅₄H₆₈N₄O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: 13.6 percent / sulfuric acid/silica gel; water / dioxane / 0.17 h

2.1: 81.7 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 0 - 20 °C

3.1: ammonium formate / Pd/C / methanol; ethyl acetate / 2 h / Heating

4.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

5.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

5.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

6.1: thiocresol / 2 h / 110 °C

6.2: tributyltin hydride; 2,2'-diazobisisobutyronitrile / toluene / 24 h / Heating

6.3: H₂; triethylamine / Pd(OH)2/C / ethyl acetate / 1 h

7.1: 1.231 g / triethylamine; potassium carbonate / acetone / 15 h

8.1: tert-butyl hypochlorite; triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

9.1: tetrafluoroboric acid-dimethyl ether copmlex; silver tetrafluoroborate / acetone / 1 h / -10 °C

10.1: 4.2 percent / KBH₄ / acetic acid / 0.5 h / 0 °C

11.1: 0.045 g / aq. hydrochloric acid / methanol

With hydrogenchloride; dmap; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; sulfuric acid; p-toluenesulfonylanhydride; water; ammonium formate; silica gel; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; para-thiocresol; tetrafluoroboric acid dimethyl ether complex; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; acetone;
DOI:10.1021/jo000250y

Reference yield:

: 362517-09-7
(3aR,4S,5S,11bS)-dimethyl 3-benzyl-2,3,3a,4,5,7-hexahydro-4-[(2S)-2-ethyl-2,3-(isopropylidenedioxy)propyl]-1H-pyrrolo[2,3-d]carbazole-5,6-dicarboxylate

: 362516-95-8
C₅₄H₆₈N₄O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: 81.7 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 0 - 20 °C

2.1: ammonium formate / Pd/C / methanol; ethyl acetate / 2 h / Heating

3.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

4.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

4.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

5.1: thiocresol / 2 h / 110 °C

5.2: tributyltin hydride; 2,2'-diazobisisobutyronitrile / toluene / 24 h / Heating

5.3: H₂; triethylamine / Pd(OH)2/C / ethyl acetate / 1 h

6.1: 1.231 g / triethylamine; potassium carbonate / acetone / 15 h

7.1: tert-butyl hypochlorite; triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

8.1: tetrafluoroboric acid-dimethyl ether copmlex; silver tetrafluoroborate / acetone / 1 h / -10 °C

9.1: 4.2 percent / KBH₄ / acetic acid / 0.5 h / 0 °C

10.1: 0.045 g / aq. hydrochloric acid / methanol

With hydrogenchloride; dmap; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; p-toluenesulfonylanhydride; ammonium formate; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; para-thiocresol; tetrafluoroboric acid dimethyl ether complex; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; acetone;
DOI:10.1021/jo000250y