di(tert-butyl)fluorophenylsilane

Base Information

• Chemical Name: di(tert-butyl)fluorophenylsilane
• CAS No.: 165554-49-4
• Molecular Formula: C₁₄H₂₃FSi
• Molecular Weight: 238.421
• Mol file: 165554-49-4.mol

Synonyms:di(tert-butyl)fluorophenylsilane

Chemical Property of di(tert-butyl)fluorophenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di(tert-butyl)fluorophenylsilane

There total 2 articles about di(tert-butyl)fluorophenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

di-tert-butyliodophenylsilane (359875-86-8) → di(tert-butyl)fluorophenylsilane (165554-49-4)

Guidance literature:

With tetrabutylammonium triphenyldifluorostannate; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1002/anie.200600795

Reference yield:

di-tert-butylphenylsilane (18415-17-3) → di(tert-butyl)fluorophenylsilane (165554-49-4)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine chloride / CH₂Cl₂ / 0.17 h / 20 °C

2: 87 percent / tetrabutylammonium difluorotriphenylstannate / CH₂Cl₂ / 48 h / 20 °C

With Iodine monochloride; tetrabutylammonium triphenyldifluorostannate; In dichloromethane;

DOI:10.1002/anie.200600795

Reference yield: 60.0%

di(tert-butyl)fluorophenylsilane (165554-49-4) → Di-tert-butylphenylsilylhydrazin (180508-31-0)

Guidance literature:

With n-butyllithium; hydrazine; In tetrahydrofuran; hexane; 1.) room temperature, 24 h, 2.) reflux, 36 h;

DOI:10.1080/10426509608029646

upstream raw materials:

di-tert-butyliodophenylsilane

di-tert-butylphenylsilane

Downstream raw materials:

Di-tert-butylphenylsilylhydrazin