Technology Process of 1,3-bis(bromoethynyl)-2-(4-methoxybenzyloxy)benzene
There total 5 articles about 1,3-bis(bromoethynyl)-2-(4-methoxybenzyloxy)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; silver nitrate;
In
acetone;
for 1h;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.01.045
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 36 h / 20 °C / Inert atmosphere
2: potassium hydroxide / methanol / 0.58 h
3: N-Bromosuccinimide; silver nitrate / acetone / 1 h / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; silver nitrate; triethylamine; potassium hydroxide;
In
methanol; acetone;
DOI:10.1016/j.bmc.2012.01.045
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide; iodine / water / 20 °C
2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 60 °C / Inert atmosphere
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 36 h / 20 °C / Inert atmosphere
4: potassium hydroxide / methanol / 0.58 h
5: N-Bromosuccinimide; silver nitrate / acetone / 1 h / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; dihydrogen peroxide; iodine; potassium carbonate; silver nitrate; triethylamine; potassium iodide; potassium hydroxide;
In
methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.01.045
