4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide
CAS No.:475292-58-1
Molecular Formula:C₁₇H₂₃NO₃S
Molecular Weight:321.441
Hs Code.:

Synonyms:4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Suppliers and Price of 4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

There total 3 articles about 4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 686273-51-8
N-(3-hydroxypropyl)-4-methyl-N-(2-cyclopentylidene-ethyl)benzenesulfonamide

: 475292-58-1
4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; pyridinium chlorochromate; 4 A molecular sieve; In dichloromethane; for 1.25h;
DOI:10.1021/jo052532+

Reference yield:

: 13379-98-1
3-[N-(4-methylphenylsulfonyl)amino]propan-1-ol

: 475292-58-1
4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / cesium carbonate / dimethylformamide / 1.5 h

2: 85 percent / pyridinium chlorochromate; N-methylmorpholine N-oxide; tetrapropylammonium perruthenate / molecular sieves 4 Angstroem / CH₂Cl₂ / 1.25 h

With tetrapropylammonium perruthennate; caesium carbonate; 4-methylmorpholine N-oxide; pyridinium chlorochromate; 4 A molecular sieve; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052532+

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 475292-58-1
4-methyl-N-(2-cyclopentylidene-ethyl)-N-(3-oxopropyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

2: 65 percent / cesium carbonate / dimethylformamide / 1.5 h

3: 85 percent / pyridinium chlorochromate; N-methylmorpholine N-oxide; tetrapropylammonium perruthenate / molecular sieves 4 Angstroem / CH₂Cl₂ / 1.25 h

With tetrapropylammonium perruthennate; caesium carbonate; 4-methylmorpholine N-oxide; triethylamine; pyridinium chlorochromate; 4 A molecular sieve; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052532+