Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

Base Information

Chemical Name:Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester
CAS No.:203439-58-1
Molecular Formula:C₃₀H₂₈O₆
Molecular Weight:484.549
Hs Code.:

Synonyms:Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

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Chemical Property of Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

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Technology Process of Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

There total 6 articles about Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 39720-27-9
4-acetoxybenzyl chloride

: 203441-50-3
2-(3-Cyclopentyloxy-4-methoxy-phenyl)-indan-1,3-dione

: 203439-58-1
Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

Guidance literature:: With potassium carbonate; sodium iodide; In acetone; for 1h; Heating;
DOI:10.1021/jm970575f

Reference yield:

: 85-44-9
phthalic anhydride

: 203439-58-1
Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOAc, 2.) NaOMe / 1.) 200 deg C, 4 h, 2.) MeOH, reflux, 0.5 h

2: 74 percent / K₂CO₃, NaI / acetone / 1 h / Heating

With sodium methylate; sodium acetate; potassium carbonate; sodium iodide; In acetone;
DOI:10.1021/jm970575f

Reference yield:

: 1131-94-8
homoisovanillic acid

: 203439-58-1
Acetic acid 4-[2-(3-cyclopentyloxy-4-methoxy-phenyl)-1,3-dioxo-indan-2-ylmethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / conc. H₂SO₄ / 2 h / Heating

2: 89 percent / DEAD, Ph₃P / tetrahydrofuran / Ambient temperature

3: 95 percent / 1 N NaOH / methanol / Ambient temperature

4: 1.) NaOAc, 2.) NaOMe / 1.) 200 deg C, 4 h, 2.) MeOH, reflux, 0.5 h

5: 74 percent / K₂CO₃, NaI / acetone / 1 h / Heating

With sodium hydroxide; sulfuric acid; sodium methylate; sodium acetate; potassium carbonate; triphenylphosphine; sodium iodide; diethylazodicarboxylate; In tetrahydrofuran; methanol; acetone;
DOI:10.1021/jm970575f