(RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide

Base Information

• Chemical Name: (RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide
• CAS No.: 1173713-04-6
• Molecular Formula: C₁₁H₁₄BrNO₃S
• Molecular Weight: 320.207

Synonyms:(RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide

Chemical Property of (RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide

Chemical Property:

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Technology Process of (RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide

There total 1 articles about (RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

(RS)-N-(ethoxycarbonyl)-S-methyl-S-(m-tolyl)sulphoximide (1173713-03-5) → (RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide (1173713-04-6)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 5h; Heating / reflux;

Reference yield: 97.0%

4-(Isopropylamino)-6-methoxyquinazolin-7-ol (1173713-25-1) + (RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide (1173713-04-6) → (RS)-N-(ethoxycarbonyl)-S-[3-({[4-(isopropylamino)-6-methoxyquinazolin-7-yl]oxy}methyl)phenyl]-S-methylsulphoximide (1173712-87-2)

Guidance literature:

With caesium carbonate; In acetone; for 3h; Heating / reflux;

Reference yield: 86.0%

(RS)-S-[3-(bromomethyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide (1173713-04-6) + ethyl 7-hydroxy-4-(thiazol-2-ylamino)quinazoline-6-carboxylate acetate → Ethyl 7-({(RS)-3-[N-(ethoxycarbonyl)-S-methylsulphonimidoyl]benzyl}oxy)-4-(thiazol-2-ylamino)quinazoline-6-carboxylate (1173712-85-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; acetone; for 7h; Heating / reflux;

upstream raw materials:

(RS)-N-(ethoxycarbonyl)-S-methyl-S-(m-tolyl)sulphoximide

Downstream raw materials:

(RS)-N-(ethoxycarbonyl)-S-[3-({[4-(isopropylamino)quinazolin-7-yl]oxy}methyl)-phenyl]-S-methylsulphoximide

(RS)-N-(ethoxycarbonyl)-S-[3-({[4-(isopropylamino)-6-methoxyquinazolin-7-yl]oxy}methyl)phenyl]-S-methylsulphoximide

(RS)-S-[3-({[6-cyano-4-(isopropylamino)quinazolin-7-yl]oxy}methyl)phenyl]-N-(ethoxycarbonyl)-S-methylsulphoximide

ethyl 5-cyano-4-{(E/Z)-[(dimethylamino)methylene]amino}-2-({(RS)-3-[N-(ethoxycarbonyl)-S-methylsulphonimidoyl]benzyl}oxy)benzoate

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