1,4,6,7-TETRAHYDROIMIDAZO[4,5-E][1,4]DIAZEPINE-5,8-DIONE

Base Information

• Chemical Name: 1,4,6,7-TETRAHYDROIMIDAZO[4,5-E][1,4]DIAZEPINE-5,8-DIONE
• CAS No.: 119584-65-5
• Molecular Formula: C₆H₆N₄O₂
• Molecular Weight: 166.139
• Hs Code.: 2933990090
• Mol file: 119584-65-5.mol

Synonyms:Imidazo[4,5-e][1,4]diazepine-5,8-dione,1,4,6,7-tetrahydro- (9CI); NSC 625659

Chemical Property of 1,4,6,7-TETRAHYDROIMIDAZO[4,5-E][1,4]DIAZEPINE-5,8-DIONE

Chemical Property:

• PSA: 86.88000
• LogP: -0.44160

Purity/Quality:

98%min ^*data from raw suppliers

1,4,6,7-Tetrahydroimidazo[4,5-e][1,4]diazepine-5,8-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4,6,7-TETRAHYDROIMIDAZO[4,5-E][1,4]DIAZEPINE-5,8-DIONE

There total 11 articles about 1,4,6,7-TETRAHYDROIMIDAZO[4,5-E][1,4]DIAZEPINE-5,8-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3-benzyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (133124-68-2) → 4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-65-5)

Guidance literature:

With hydrogen; acetic acid; under 760 Torr; Ambient temperature;

DOI:10.1007/BF00767004

Reference yield: 72.0%

1-benzyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-61-1) → 4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-65-5)

Guidance literature:

With hydrogen; palladium dihydroxide; In acetic acid; for 16h; under 2068.6 Torr; Ambient temperature;

DOI:10.1002/jhet.5570250426

Reference yield: 68.0%

5(4)-amino-4(5)-(N-carboxymethyl)carbamoyl-1(3)H-imidazole (132459-08-6) → 4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-65-5)

Guidance literature:

With acetic acid; for 3h; Heating;

upstream raw materials:

5⁽⁴⁾-amino-4⁽⁵⁾-(N-carboxymethyl)carbamoyl-1⁽³⁾H-imidazole

5⁽⁴⁾-amino-4⁽⁵⁾-(N-methoxycarbonylmethyl)carbamoyl-1⁽³⁾H-imidazole

5⁽⁴⁾-nitro-4⁽⁵⁾-(N-methoxycarbonylmethyl)carbamoyl-1⁽³⁾H-imidazole

1-benzyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione