Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid
CAS No.:92052-27-2
Molecular Formula:C₄₆H₅₈N₂O₁₉*H₃N
Molecular Weight:959.999
Hs Code.:

Benzyl-O-<ammonium-(3-desoxy-α-D-manno-2-octulopyranosyl)onat>-(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Synonyms:Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

There total 5 articles about Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 92070-32-1,92125-37-6
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92052-27-2
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: With sodium hydroxide; Dowex 50 W; ammonia; hydrogen cation; In methanol; for 18h;

Reference yield:

: 92052-20-5
Benzyl-6-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92052-27-2
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: Hg(CN)2, molecular sieve (4 Angstroem) / nitromethane / 1.) 60 deg C, 2 h, 2.) room temp., 18 h

2: 13 percent / pyridine / 18 h / 0 °C

3: 90 percent / 0.5 N NaOH; Dowex 50 W, H⁽¹⁺⁾-form); NH₃ / methanol / 18 h

With sodium hydroxide; 4 A molecular sieve; Dowex 50 W; ammonia; mercury(II) cyanide; hydrogen cation; In pyridine; methanol; nitromethane;

Reference yield:

: 92052-19-2
Benzyl-6-O-(2-acetamido-2-desoxy-β-D-glucopyranosyl)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92052-27-2
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / p-toluenesulfonic acid / acetonitrile / 144 h

2: Hg(CN)2, molecular sieve (4 Angstroem) / nitromethane / 1.) 60 deg C, 2 h, 2.) room temp., 18 h

3: 13 percent / pyridine / 18 h / 0 °C

4: 90 percent / 0.5 N NaOH; Dowex 50 W, H⁽¹⁺⁾-form); NH₃ / methanol / 18 h

With sodium hydroxide; 4 A molecular sieve; Dowex 50 W; ammonia; mercury(II) cyanide; hydrogen cation; toluene-4-sulfonic acid; In pyridine; methanol; nitromethane; acetonitrile;