Imidazo[4,5-e][1,4]diazepine-5,8-dione, 1,4,6,7-tetrahydro-4,7-dimethy l-

Base Information

• Chemical Name: Imidazo[4,5-e][1,4]diazepine-5,8-dione, 1,4,6,7-tetrahydro-4,7-dimethy l-
• CAS No.: 119584-58-6
• Molecular Formula: C₈H₁₀N₄O₂
• Molecular Weight: 194.193
• Mol file: 119584-58-6.mol

Synonyms:Imidazo[4,5-e][1,4]diazepine-5,8-dione,1,4,6,7-tetrahydro-4,7-dimethyl- (9CI); 4,7-Dimethyl-1,4,6,7-tetrahydroimidazo[4,5-e][1,4]diazepine-5,8-dione;NSC 625660

Chemical Property of Imidazo[4,5-e][1,4]diazepine-5,8-dione, 1,4,6,7-tetrahydro-4,7-dimethy l-

Chemical Property:

• PSA: 69.30000
• LogP: -0.53900

Purity/Quality:

3,4,6,7-tetrahydro-4,7-dimethyl-Imidazo[4,5-e][1,4]diazepine-5,8-dione 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Imidazo[4,5-e][1,4]diazepine-5,8-dione, 1,4,6,7-tetrahydro-4,7-dimethy l-

There total 4 articles about Imidazo[4,5-e][1,4]diazepine-5,8-dione, 1,4,6,7-tetrahydro-4,7-dimethy l- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-benzyl-4,7-dimethyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-66-6) → 1,4-dimethyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-58-6)

Guidance literature:

With hydrogen; palladium;

DOI:10.1007/BF00473883

Reference yield:

7-benzyltheophylline (1807-85-8) → 1,4-dimethyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-58-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 38 percent / 6M aq. NaOH / ethanol / 16 h / Heating

2: 1.)K₂CO₃ 2.)EtONa / 1.)CHCl₃, r.t., 4 h 2.)EtOH, r.t., 2 h

3: 82 percent / H₂ / 20percent Pd(OH)2/C / acetic acid / 16 h / 2068.6 Torr / Ambient temperature

With sodium hydroxide; hydrogen; sodium ethanolate; potassium carbonate; palladium dihydroxide; In ethanol; acetic acid;

DOI:10.1002/jhet.5570250426

Reference yield:

N-methyl-1-benzyl-4-methylaminoimidazole-5-carboxamide (53525-62-5) → 1,4-dimethyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione (119584-58-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.)K₂CO₃ 2.)EtONa / 1.)CHCl₃, r.t., 4 h 2.)EtOH, r.t., 2 h

2: 82 percent / H₂ / 20percent Pd(OH)2/C / acetic acid / 16 h / 2068.6 Torr / Ambient temperature

With hydrogen; sodium ethanolate; potassium carbonate; palladium dihydroxide; In acetic acid;

DOI:10.1002/jhet.5570250426

upstream raw materials:

1-benzyl-4,7-dimethyl-4,5,7,8-tetrahydro-6H-imidazo<4,5-e><1,4>diazepine-5,8-dione

7-benzyltheophylline

N-methyl-1-benzyl-4-methylaminoimidazole-5-carboxamide

3-Benzyl-5-[(2-chloro-acetyl)-methyl-amino]-3H-imidazole-4-carboxylic acid methylamide

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