benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

Base Information

Chemical Name:benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside
CAS No.:74247-61-3
Molecular Formula:C₂₉H₃₁NO₉S
Molecular Weight:569.632
Hs Code.:

Synonyms:benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

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Chemical Property of benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

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Technology Process of benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

There total 3 articles about benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-24-7
acetic anhydride

: 74247-60-2
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

: 74247-61-3
benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

Guidance literature:: In pyridine; at 45 ℃; for 3h;
DOI:10.1016/S0008-6215(00)84865-X

Reference yield:

: 42890-17-5
benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-β-D-glucofuranoside

: 74247-61-3
benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 0.2M aqueous sodium metaperiodate / methanol / 2 h / 0 °C

2: 82 percent / pyridine / 5 h / Ambient temperature

3: 83 percent / pyridine / 3 h / 45 °C

With sodium periodate; In pyridine; methanol;
DOI:10.1016/S0008-6215(00)84865-X

Reference yield:

: 58886-40-1
benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 74247-61-3
benzyl 3-O-acetyl-2-(benzyloxycarbonylamino)-2-deoxy-5-O-tosyl-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / aq. acetic acid / 3 h / 40 °C

2: 83 percent / 0.2M aqueous sodium metaperiodate / methanol / 2 h / 0 °C

3: 82 percent / pyridine / 5 h / Ambient temperature

4: 83 percent / pyridine / 3 h / 45 °C

With sodium periodate; In pyridine; methanol; acetic acid;
DOI:10.1016/S0008-6215(00)84865-X