N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

Base Information

Chemical Name:N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide
CAS No.:1584736-27-5
Molecular Formula:C₂₀H₂₁NO₅
Molecular Weight:355.39
Hs Code.:

Synonyms:N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

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Chemical Property of N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

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Technology Process of N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

There total 9 articles about N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 3-(allyloxy)-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 4-methoxy-N-(2-methoxyacetyl)-benzamide

: 1584736-27-5
N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

: C₂₀H₂₁NO₅

Guidance literature:: With tetrabutylammonium triphenyldifluorosilicate; In acetonitrile; at 65 ℃; Flow reactor;
DOI:10.1021/acs.orglett.8b03392

Reference yield:

: 3424-93-9
4-methoxyphenylacetamide

: 1584736-27-5
N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / 60 °C / Sealed tube

2: tetrabutylammonium triphenyldifluorosilicate / acetonitrile / 65 °C / Flow reactor

With pyridine; tetrabutylammonium triphenyldifluorosilicate; In acetonitrile;
DOI:10.1021/acs.orglett.8b03392

Reference yield:

: 3-hydroxy-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1584736-27-5
N-(3-(allyloxy)-2-(4-methoxybenzoyl)phenyl)-2-methoxyacetamide

: C₂₀H₂₁NO₅

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; potassium phosphate / water / 1 h / 23 °C

2: tetrabutylammonium triphenyldifluorosilicate / acetonitrile / 65 °C / Flow reactor

With potassium phosphate; tetrabutylammomium bromide; tetrabutylammonium triphenyldifluorosilicate; In water; acetonitrile;
DOI:10.1021/acs.orglett.8b03392