C₃₇H₆₀O₉Si

Base Information

Chemical Name:C₃₇H₆₀O₉Si
CAS No.:1293966-71-8
Molecular Formula:C₃₇H₆₀O₉Si
Molecular Weight:676.963
Hs Code.:

C<sub>37</sub>H<sub>60</sub>O<sub>9</sub>Si

Synonyms:C₃₇H₆₀O₉Si

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Chemical Property of C₃₇H₆₀O₉Si

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Technology Process of C₃₇H₆₀O₉Si

There total 25 articles about C₃₇H₆₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₆H₆₅F₃O₁₀SSi

: 1293966-71-8
C₃₇H₆₀O₉Si

Guidance literature:: With sodium tetrahydroborate; sodium hydrogencarbonate; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol2007296

Reference yield:

: 1255763-55-3
C₂₅H₄₂O₅Si

: 1293966-71-8
C₃₇H₆₀O₉Si

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

3: sodium tetrahydroborate; sodium hydrogencarbonate / acetonitrile / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; acetonitrile; 1: Mitsunobu reaction / 2: Pummerer rearrangement;
DOI:10.1021/ol2007296

Reference yield:

: 1255763-92-8
C₁₆H₂₂O₃

: 1293966-71-8
C₃₇H₆₀O₉Si

Guidance literature:: Multi-step reaction with 7 steps

1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere

2: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere

3: Inert atmosphere

4: lithium hydroperoxide / Inert atmosphere

5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

7: sodium tetrahydroborate; sodium hydrogencarbonate / acetonitrile / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; lithium hydroperoxide; dihydrogen peroxide; sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 1: Aldol condensation / 5: Mitsunobu reaction / 6: Pummerer rearrangement;
DOI:10.1021/ol2007296