(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

Base Information

Chemical Name:(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride
CAS No.:1033706-61-4
Molecular Formula:C₆₀H₆₁FO₁₅Si
Molecular Weight:1069.22
Hs Code.:

Synonyms:(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

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Chemical Property of (2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

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Technology Process of (2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

There total 1 articles about (2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1033706-60-3
2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

: 1033706-61-4
(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

Guidance literature:: 2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside; With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

With pyridine; trifluoromethylsulfonic anhydride; hydrogen fluoride; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at -78 - 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol800530u

Reference yield: 89.0%

: 1033706-61-4
(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

: 1033706-62-5
(2,3,5-tri-O-benzoyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

Guidance literature:: With pyridine; hydrogen fluoride; water; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol800530u

Reference yield: 62.0%

: 1033706-61-4
(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

: 1033706-59-0
2'-(benzyloxycarbonyl)benzyl (2,3,5-tri-O-benzoyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

: 2'-(benzyloxycarbonyl)benzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl)-(1->6)-(2,3,5-tri-O-benzoyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

Guidance literature:: 2'-(benzyloxycarbonyl)benzyl (2,3,5-tri-O-benzoyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside; With silver perchlorate; tin(ll) chloride; In diethyl ether; at -10 ℃; for 0.166667h; Inert atmosphere; Molecular sieve;

(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride; In diethyl ether; at -10 - 0 ℃; Inert atmosphere;
DOI:10.1021/ol800530u