Ethanone, 1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3alpha,4alpha,5beta)- (9CI)

Base Information

Chemical Name:Ethanone, 1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3alpha,4alpha,5beta)- (9CI)
CAS No.:119232-93-8
Molecular Formula:C₉H₁₃FO₄
Molecular Weight:204.198
Hs Code.:
Mol file:119232-93-8.mol

Synonyms:Ethanone,1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3a,4a,5b)- (9CI); Ethanone,1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3a,4a,5b)-(?à)-

Suppliers and Price of Ethanone, 1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3alpha,4alpha,5beta)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethanone, 1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3alpha,4alpha,5beta)- (9CI)

Chemical Property:

PSA：52.60000
LogP:0.69670

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3alpha,4alpha,5beta)- (9CI)

There total 8 articles about Ethanone, 1-[5-(acetyloxy)tetrahydro-4-methyl-3-furanyl]-2-fluoro-, (3alpha,4alpha,5beta)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119232-90-5
(3R,4S)-3-Benzyloxymethyl-1-fluoro-4-methyl-hex-5-en-2-one

: 119232-93-8
Acetic acid (3R,4R)-4-(2-fluoro-acetyl)-3-methyl-tetrahydro-furan-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methylmorpholine N-oxide / OsO₄ / tetrahydrofuran; H₂O

2: H₂ / Pd/C / ethyl acetate

3: NaIO₄ / H₂O

4: pyridine

With pyridine; sodium periodate; hydrogen; 4-methylmorpholine N-oxide; palladium on activated charcoal; osmium(VIII) oxide; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/S0040-4039(00)86049-9

Reference yield:

: 119232-90-5
(3R,4R)-3-Benzyloxymethyl-1-fluoro-4-methyl-hex-5-en-2-one

: 119232-93-8
Acetic acid (2R,3S,4R)-4-(2-fluoro-acetyl)-3-methyl-tetrahydro-furan-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 4-methylmorpholine N-oxide / OsO₄ / tetrahydrofuran; H₂O

2: 78 percent / H₂ / Pd/C / ethyl acetate

3: 50 percent / NaIO₄ / H₂O

4: pyridine

With pyridine; sodium periodate; hydrogen; 4-methylmorpholine N-oxide; palladium on activated charcoal; osmium(VIII) oxide; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/S0040-4039(00)86049-9

Reference yield:

: 119232-91-6
(3R,4S)-3-Benzyloxymethyl-1-fluoro-5,6-dihydroxy-4-methyl-hexan-2-one

: 119232-93-8
Acetic acid (2R,3S,4R)-4-(2-fluoro-acetyl)-3-methyl-tetrahydro-furan-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / H₂ / Pd/C / ethyl acetate

2: 50 percent / NaIO₄ / H₂O

3: pyridine

With pyridine; sodium periodate; hydrogen; palladium on activated charcoal; In water; ethyl acetate;
DOI:10.1016/S0040-4039(00)86049-9