<1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

Base Information

Chemical Name:<1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine
CAS No.:182509-48-4
Molecular Formula:C₁₂H₂₂N₂O₃
Molecular Weight:242.318
Hs Code.:

Synonyms:<1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

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Chemical Property of <1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

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Technology Process of <1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

There total 1 articles about <1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 182509-48-4
<1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

Guidance literature:: With magnesium sulfate; In diethyl ether; for 1h; Ambient temperature;
DOI:10.1016/0957-4166(96)00124-3

Reference yield:

: 182509-48-4
<1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

: 178363-61-6
<<(1R)-1-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>-2-phenyl>ethyl>amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Et₂O, from -60 deg C to RT, 3 h, 2.) Et₂O, RT, 17 h

2: 25 percent / Li/NH₃ / tetrahydrofuran / 1.5 h / -70 - -33 °C

3: 86 percent / 2N aq. NaOH / ethanol / 3 h / Heating

With sodium hydroxide; ammonia; lithium; In tetrahydrofuran; ethanol;
DOI:10.1016/0957-4166(96)00124-3

Reference yield:

: 182509-48-4
<1-<<<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methylidene>amino>-2-(2S)-methoxymethyl>pyrrolidine

: 178363-60-5
<<(1R)-1-<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>-2-phenyl>ethyl>carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₂O, from -60 deg C to RT, 3 h, 2.) Et₂O, RT, 17 h

2: 25 percent / Li/NH₃ / tetrahydrofuran / 1.5 h / -70 - -33 °C

With ammonia; lithium; In tetrahydrofuran;
DOI:10.1016/0957-4166(96)00124-3