N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester
CAS No.:295800-31-6
Molecular Formula:C₃₁H₃₇N₃O₄
Molecular Weight:515.652
Hs Code.:

<i>N</i>'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-<i>tert</i>-butyl-9<i>H</i>-fluoren-9-ylmethyl ester

Synonyms:N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

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Chemical Property of N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

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Technology Process of N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

There total 4 articles about N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 287381-48-0
N'-(2-methoxy-5-nitro-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

: 295800-31-6
N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

Guidance literature:: With hydrogen; 10percent Pd/C; In tetrahydrofuran; methanol; for 2h;
DOI:10.1021/ja001142w

Reference yield:

: 40751-89-1
2-methoxy-5-nitrobenzoic acid

: 295800-31-6
N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 0.5 h

2: H₂ / 10percent Pd/C / methanol; tetrahydrofuran / 2 h

With pyridine; hydrogen; 10percent Pd/C; In tetrahydrofuran; methanol; dichloromethane; 1: Acylation / 2: Reduction;
DOI:10.1021/ja001142w

Reference yield:

: 287381-46-8
2,7-di-tert-butyl-9-fluorenylmethoxycarbonyl chloride

: 295800-31-6
N'-(5-amino-2-methoxy-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / hydrazine / diethyl ether / 3 h

2: pyridine / CH₂Cl₂ / 0.5 h

3: H₂ / 10percent Pd/C / methanol; tetrahydrofuran / 2 h

With pyridine; hydrogen; hydrazine; 10percent Pd/C; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 1: Acylation / 2: Acylation / 3: Reduction;
DOI:10.1021/ja001142w