(1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol

Base Information

• Chemical Name: (1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol
• CAS No.: 1258542-72-1
• Molecular Formula: C₂₀H₃₂N₂O₉S₂
• Molecular Weight: 508.614

Synonyms:(1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol

Chemical Property of (1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol

Chemical Property:

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Technology Process of (1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol

There total 1 articles about (1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N-Boc-L-methionine sulfone (60280-45-7) + (1R,2R)-2-amino-1-<4-(methylsulphonyl)phenyl>-1,3-propanediol (51458-28-7) → (1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol (1258542-72-1)

Guidance literature:

With 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1016/j.bmc.2010.09.045

Reference yield: 100.0%

(1R,2R)-1-(4-methylsulfonylphenyl)-2-(Nα-Boc-L-methionylsulfone-amido)-1,3-propadiol (1258542-72-1) → (1R,2R)-1-(4-methylsulfonylphenyl)-2-(L-methionyl-sulfone-amido)-1,3-propadiol hydrochloride (1258542-80-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.666667h;

DOI:10.1016/j.bmc.2010.09.045

upstream raw materials:

N-Boc-L-methionine sulfone

(1R,2R)-2-amino-1-<4-(methylsulphonyl)phenyl>-1,3-propanediol

Downstream raw materials:

(1R,2R)-1-(4-methylsulfonylphenyl)-2-(L-methionyl-sulfone-amido)-1,3-propadiol hydrochloride

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