C₂₂H₂₀F₂N₂O₅

Base Information

Chemical Name:C₂₂H₂₀F₂N₂O₅
CAS No.:1277102-31-4
Molecular Formula:C₂₂H₂₀F₂N₂O₅
Molecular Weight:430.408
Hs Code.:

C<sub>22</sub>H<sub>20</sub>F<sub>2</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₂H₂₀F₂N₂O₅

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Chemical Property of C₂₂H₂₀F₂N₂O₅

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Technology Process of C₂₂H₂₀F₂N₂O₅

There total 6 articles about C₂₂H₂₀F₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1277102-29-0
(2R,3R)-2,3-difluoro-4-phthalimidobutyric acid

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 1277102-31-4
C₂₂H₂₀F₂N₂O₅

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201003320

Reference yield:

: C₁₇H₁₃NO₅S

: 1277102-31-4
C₂₂H₂₀F₂N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: sodium periodate; ruthenium(III) trichloride hydrate / dichloromethane; water; acetonitrile / 0.08 h / 0 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; acetonitrile / 1 h / 0 °C / Molecular sieve; Inert atmosphere

3: sulfuric acid / tetrahydrofuran; water / 20 °C / Inert atmosphere

4: (bis-(2-methoxyethyl)amino)sulfur trufluoride / 70 °C / Inert atmosphere

5: sodium periodate; ruthenium(III) trichloride hydrate / dichloromethane; water; acetonitrile / 96 h / 20 °C / Inert atmosphere

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / water; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With sodium periodate; ruthenium(III) trichloride hydrate; sulfuric acid; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201003320

Reference yield:

: 1277102-25-6
C₁₇H₁₅NO₄

: 1277102-31-4
C₂₂H₂₀F₂N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine; thionyl chloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: sodium periodate; ruthenium(III) trichloride hydrate / dichloromethane; water; acetonitrile / 0.08 h / 0 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran; acetonitrile / 1 h / 0 °C / Molecular sieve; Inert atmosphere

4: sulfuric acid / tetrahydrofuran; water / 20 °C / Inert atmosphere

5: (bis-(2-methoxyethyl)amino)sulfur trufluoride / 70 °C / Inert atmosphere

6: sodium periodate; ruthenium(III) trichloride hydrate / dichloromethane; water; acetonitrile / 96 h / 20 °C / Inert atmosphere

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / water; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With pyridine; sodium periodate; thionyl chloride; ruthenium(III) trichloride hydrate; sulfuric acid; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201003320