2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide

Base Information

• Chemical Name: 2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide
• CAS No.: 1254214-32-8
• Molecular Formula: C₁₉H₂₅N₇O₂
• Molecular Weight: 383.453

Synonyms:2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide

Chemical Property of 2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide

Chemical Property:

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Technology Process of 2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide

There total 1 articles about 2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl 3-((2-(3-acetamidophenylamino)-5-carbamoylpyrimidin-4-ylamino)methyl)piperidine-1-carboxylate (1254214-31-7) → 2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide (1254214-32-8)

Guidance literature:

With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In methanol; water; for 18h;

Reference yield:

2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide (1254214-32-8) + para-fluorophenyl isocyanate (1195-45-5) → 2-(3-acetamidophenylamino)-4-((1-(4-fluorophenylcarbamoyl)piperidin-3-yl)methylamino)pyrimidine-5-carboxamide (1254214-34-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

2-(3-acetamidophenylamino)-4-(piperidin-3-ylmethylamino)pyrimidine-5-carboxamide (1254214-32-8) + acetic anhydride (108-24-7) → 2-(3-acetamidophenylamino)-4-((1-acetylpiperidin-3-yl)methylamino)pyrimidine-5-carboxamide (1254214-35-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;

upstream raw materials:

benzyl 3-((2-(3-acetamidophenylamino)-5-carbamoylpyrimidin-4-ylamino)methyl)piperidine-1-carboxylate

Downstream raw materials:

2-(3-acetamidophenylamino)-4-((1-acetylpiperidin-3-yl)methylamino)pyrimidine-5-carboxamide

2-(3-acetamidophenylamino)-4-((1-(methylsulfonyl)piperidin-3-yl)methylamino)pyrimidine-5-carboxamide

2-(3-acetamidophenylamino)-4-((1-carbamoylpiperidin-3-yl)methylamino)pyrimidine-5-carboxamide

2-(3-acetamidophenylamino)-4-((1-(4-fluorophenylcarbamoyl)piperidin-3-yl)methylamino)pyrimidine-5-carboxamide

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