1--2-benzoylnaphthalene

Base Information

• Chemical Name: 1--2-benzoylnaphthalene
• CAS No.: 154848-94-9
• Molecular Formula: C₁₉H₁₄BrNO₂
• Molecular Weight: 368.23

Synonyms:1--2-benzoylnaphthalene

Chemical Property of 1--2-benzoylnaphthalene

Chemical Property:

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Technology Process of 1--2-benzoylnaphthalene

There total 3 articles about 1--2-benzoylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-amino-2-benzoylnaphthalene (153684-50-5) + 2-Bromoacetyl bromide (598-21-0) → 1--2-benzoylnaphthalene (154848-94-9)

Guidance literature:

With sodium hydrogencarbonate; In chloroform; at 0 ℃; for 0.5h;

DOI:10.1021/jm00032a007

Reference yield:

1-amino-2-naphthalenecarbonitrile (3100-67-2) → 1--2-benzoylnaphthalene (154848-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) 2 N aq. HCl / 1.) Et₂O, reflux, 1 h, 2.) Et₂O, 30 deg C, 2 h

2: 94 percent / NaHCO₃ / CHCl₃ / 0.5 h / 0 °C

With hydrogenchloride; sodium hydrogencarbonate; In chloroform;

DOI:10.1021/jm00032a007

Reference yield:

phenylmagnesium bromide → 1--2-benzoylnaphthalene (154848-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) 2 N aq. HCl / 1.) Et₂O, reflux, 1 h, 2.) Et₂O, 30 deg C, 2 h

2: 94 percent / NaHCO₃ / CHCl₃ / 0.5 h / 0 °C

With hydrogenchloride; sodium hydrogencarbonate; In chloroform;

DOI:10.1021/jm00032a007

upstream raw materials:

1-amino-2-benzoylnaphthalene

2-Bromoacetyl bromide

1-amino-2-naphthalenecarbonitrile

Downstream raw materials:

5-phenyl-1,3-dihydronaphtho<1,2-e><1,4>diazepin-2-one

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