1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole

Base Information

• Chemical Name: 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole
• CAS No.: 127553-37-1
• Molecular Formula: C₂₈H₂₅N₃O₇
• Molecular Weight: 515.522

Synonyms:1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole

Chemical Property of 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole

Chemical Property:

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Technology Process of 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole

There total 6 articles about 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride (4330-21-6) + 4-nitro-benzimidazole (10597-52-1) → 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-4-nitrobenzimidazole (127553-36-0) + 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole (127553-37-1)

Guidance literature:

4-nitro-benzimidazole; With sodium hydride; In acetonitrile; mineral oil; at 0 ℃; for 1h;

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride; In acetonitrile; mineral oil; at 0 - 20 ℃; for 5h;

DOI:10.1080/15257770903451579

Reference yield: 30.0%

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride (4330-21-6) + 4-nitro-benzimidazole (10597-52-1) → 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-4-nitrobenzimidazole (127553-36-0) + 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole (127553-37-1) + 1-<2-Deoxy-3,5-di-O-(4-methylbenzoyl)-α-D-erythro-pentofuranosyl>-7-nitrobenzimidazole (127553-37-1)

Guidance literature:

With potassium hydroxide; TDA-1; for 0.5h; 1.) CH₃CN, room temp., 30 min, 2.) 30 min;

DOI:10.1055/s-1989-27429

Reference yield: 30.0%

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride (4330-21-6) + 4-nitro-benzimidazole (10597-52-1) → 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-4-nitrobenzimidazole (127553-36-0) + 1-<2-Deoxy-3,5-bis-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl>-7-ntrobenzimidazole (127553-37-1) + 1-<2-Deoxy-3,5-di-O-(4-methylbenzoyl)-α-D-erythro-pentofuranosyl>-7-nitrobenzimidazole (127553-37-1)

Guidance literature:

With potassium hydroxide; TDA-1; for 0.5h; 1.) CH₃CN, room temp., 30 min, 2.) 30 min;

DOI:10.1055/s-1989-27429

upstream raw materials:

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

4-nitro-benzimidazole

7-nitro-1H-benzo[d]imidazole

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