N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

Base Information

Chemical Name:N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride
CAS No.:1608501-55-8
Molecular Formula:C₁₅H₁₄N₄O₂S₂*ClH
Molecular Weight:382.895
Hs Code.:

Synonyms:N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

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Technology Process of N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

There total 4 articles about N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: N-(4-methyl-5-(6-(phenylsulfonamido)pyridin-2-yl)thiazol-2-yl)acetamide

: 1608501-55-8
N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

Guidance literature:: With hydrogenchloride; water; at 80 ℃; for 20h;
DOI:10.1039/c3cc48391f

Reference yield:

: 19798-81-3,1184170-10-2
2-Amino-6-bromopyridine

: 1608501-55-8
N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2.5 h / 0 - 20 °C

2: palladium diacetate; tri-tert-butyl phosphine; cesium fluoride / dimethyl sulfoxide / 6 h / 140 °C

3: hydrogenchloride; water / 20 h / 80 °C

With pyridine; hydrogenchloride; tri-tert-butyl phosphine; water; palladium diacetate; cesium fluoride; In dimethyl sulfoxide;
DOI:10.1039/c3cc48391f

Reference yield:

: 1155570-12-9
N-(6-bromopyridin-2-yl)benzenesulfonamide

: 1608501-55-8
N-[6-(2-amino-4-methyl-1,3-thiazol-5-yl)pyridin-2-yl]benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; tri-tert-butyl phosphine; cesium fluoride / dimethyl sulfoxide / 6 h / 140 °C

2: hydrogenchloride; water / 20 h / 80 °C

With hydrogenchloride; tri-tert-butyl phosphine; water; palladium diacetate; cesium fluoride; In dimethyl sulfoxide;
DOI:10.1039/c3cc48391f