(Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal

Base Information

Chemical Name:(Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal
CAS No.:117672-00-1
Molecular Formula:C₁₃H₁₃ClO₂S₂
Molecular Weight:300.83
Hs Code.:

Synonyms:(Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal

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Technology Process of (Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal

There total 2 articles about (Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 117671-92-8
1-[(2S,3R)-3-(4-Chloro-phenyl)-oxiranyl]-3,3-bis-methylsulfanyl-propenone

: 117672-00-1
(Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; for 5h; Heating;
DOI:10.1055/s-1987-28112

Reference yield:

: 89812-53-3
(E)-5-(4-chlorophenyl)-1,1-bis(methylthio)penta-1,4-dien-3-one

: 117672-00-1
(Z)-2-(4-Chloro-phenyl)-3-hydroxy-5,5-bis-methylsulfanyl-penta-2,4-dienal

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 30percent H₂O₂, 3 N aq. NaOH / methanol / 6 h / Ambient temperature

2: 87 percent / BF₃*Et₂O / tetrahydrofuran / 5 h / Heating

With sodium hydroxide; boron trifluoride diethyl etherate; dihydrogen peroxide; In tetrahydrofuran; methanol;
DOI:10.1055/s-1987-28112