2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ^5,5a-carba-D-galactopyranose

Base Information

• Chemical Name: 2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ^5,5a-carba-D-galactopyranose
• CAS No.: 1225450-78-1
• Molecular Formula: C₉₁H₉₀O₁₄S
• Molecular Weight: 1439.77

Synonyms:2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ^5,5a-carba-D-galactopyranose

Chemical Property of 2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ^5,5a-carba-D-galactopyranose

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Technology Process of 2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ^5,5a-carba-D-galactopyranose

There total 1 articles about 2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ^5,5a-carba-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-acetylthio-α-Δ5,5a-carba-D-galactopyranose (1225450-77-0) → 2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ5,5a-carba-D-galactopyranose (1225450-78-1)

Guidance literature:

With hydrazinium monoacetate; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1016/j.carres.2009.12.024

Reference yield: 36.0%

allyl (methyl 2,3-di-O-(4-methoxyphenylmethyl)-4-O-trifluoromethanesulfonyl-α-D-glucopyranosid)uronate (1225450-79-2) + 2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-thio-α-Δ5,5a-carba-D-galactopyranose (1225450-78-1) → C117H120O22S (1225450-80-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

DOI:10.1016/j.carres.2009.12.024

upstream raw materials:

2,3,4-tri-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-(4-methoxyphenylmethyl)-6-O-triphenylmethyl-1-acetylthio-α-Δ^5,5a-carba-D-galactopyranose

Downstream raw materials:

C₁₁₇H₁₂₀O₂₂S

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