((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea

Base Information

Chemical Name:((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea
CAS No.:85719-53-5
Molecular Formula:C₂H₆N₂S*C₁₂H₁₅N₂O₆P
Molecular Weight:404.384
Hs Code.:

Synonyms:((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea

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Chemical Property of ((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea

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Technology Process of ((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea

There total 3 articles about ((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80082-81-1
benzyl N-[(3S)-2-oxoazetidin-3-yl]carbamate

: 85719-53-5
((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1) THF, -78 deg C; 2) -78 deg C

2: acetonitrile / Heating

With n-butyllithium; In acetonitrile;
DOI:10.1021/ja00349a084

Reference yield:

: 85710-29-8
C₁₇H₂₉N₂O₆PSi₂

: 85719-53-5
((S)-3-Benzyloxycarbonylamino-2-oxo-azetidin-1-yl)-phosphonic acid monomethyl ester; compound with 2-methyl-isothiourea

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / Heating; pH 4 (phosphate buffer)

2: 1.) n-BuLi / 1) THF, -78 deg C; 2) -78 deg C

3: acetonitrile / Heating

With n-butyllithium; water; In acetonitrile;
DOI:10.1021/ja00349a084