5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole
CAS No.:1403608-12-7
Molecular Formula:C₂₇H₃₂N₄O₃SSi
Molecular Weight:520.728
Hs Code.:

Synonyms:5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

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Technology Process of 5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

There total 5 articles about 5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₂₇H₃₂N₄OSSi

: 1403608-12-7
5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/hlca.201500267

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1403608-12-7
5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole

2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / -20 - 0 °C

4: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 6 h / 0 - 20 °C

With 1H-imidazole; hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; water; dihydrogen peroxide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; 3: Mitsunobu reaction;
DOI:10.1002/ejoc.201200241

Reference yield:

: 154491-89-1
(R)-3-(tert-butyl-diphenyl-silanyloxy)-butan-1-ol

: 1403608-12-7
5-{[(3R)-3-{[tert-butyl(diphenyl)silyl]oxy}butyl]sulfonyl}-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / -20 - 0 °C

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 6 h / 0 - 20 °C

With hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1002/ejoc.201200241