(S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

Base Information

Chemical Name:(S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide
CAS No.:267643-64-1
Molecular Formula:C₂₄H₃₁N₃O
Molecular Weight:377.53
Hs Code.:

Synonyms:(S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

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Chemical Property of (S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

Chemical Property:

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Technology Process of (S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

There total 3 articles about (S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80632-27-5
4-Toluenesulfonic acid-2-(4-cyanophenyl)ethyl ester

: 267643-57-2
(S)-N-(pyrrolidin-3-yl)-1-adamantanecarboxamide

: 267643-64-1
(S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

Guidance literature:: With potassium carbonate; In acetonitrile;
DOI:10.1016/S0960-894X(00)00492-3

Reference yield:

: 2094-72-6
1-Adamantanecarbonyl chloride

: 267643-64-1
(S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N / CH₂Cl₂

2: 88 percent / NH₂NH₂*H₂O / 10 percent Pd/C / ethanol

3: K₂CO₃ / acetonitrile

With potassium carbonate; hydrazine hydrate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; acetonitrile; 1: Acylation / 2: Hydrogenolysis / 3: Alkylation;
DOI:10.1016/S0960-894X(00)00492-3

Reference yield:

: 267643-71-0
(S)-N-(1-benzylpyrrolidin-3-yl)-1-adamantanecarboxamide

: 267643-64-1
(S)-N-(1-(2-(4-cyanophenyl)ethyl)pyrrolidin-3-yl)-1-adamantanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NH₂NH₂*H₂O / 10 percent Pd/C / ethanol

2: K₂CO₃ / acetonitrile

With potassium carbonate; hydrazine hydrate; palladium on activated charcoal; In ethanol; acetonitrile; 1: Hydrogenolysis / 2: Alkylation;
DOI:10.1016/S0960-894X(00)00492-3