benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

Base Information

Chemical Name:benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate
CAS No.:1239438-08-4
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

Synonyms:benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

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Chemical Property of benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

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Technology Process of benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

There total 1 articles about benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 3179-63-3
3-Dimethylamino-1-propanol

: 223718-30-7
3-(benzyloxycarbonyl)amino-7-hydroxy-8-methyl-2H-1-benzopyran-2-one

: 1239438-08-4
benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jm200148p

Reference yield:

: 1239438-08-4
benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

: 1239438-11-9
4-(7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamoyl)-2-(3-methylbut-2-enyl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on carbon; hydrogen / tetrahydrofuran

2: pyridine; dichloromethane / 2 h / 20 °C

With palladium on carbon; hydrogen; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/jm200148p

Reference yield:

: 1239438-08-4
benzyl 7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

: 1239438-15-3
N-(7-(3-(dimethylamino)propoxy)-8-methyl-2-oxo-2H-chromen-3-yl)-4-hydroxy-3-(3-methylbut-2-enyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on carbon; hydrogen / tetrahydrofuran

2: pyridine; dichloromethane / 2 h / 20 °C

3: triethylamine / methanol / 20 °C

With palladium on carbon; hydrogen; triethylamine; In tetrahydrofuran; pyridine; methanol; dichloromethane;
DOI:10.1021/jm200148p