Technology Process of 1-benzenesulfonyl-dodecan-6-one
There total 6 articles about 1-benzenesulfonyl-dodecan-6-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Mg / diethyl ether / 0.5 h / 25 °C
1.2: diethyl ether / 2 h / 25 °C
2.1: iodine / xylene / 4 h / Heating
3.1: ozone / methanol / 0.17 h / 0 °C
3.2: 1.04 g / NaBH4 / methanol / 0.5 h / 0 °C
4.1: 88 percent / CBr4; PPh3 / CH2Cl2 / 20 h / 0 °C
5.1: 97 percent / Celite; CrO3; sulfuric acid / acetone; H2O / 1 h / 0 °C
6.1: 85 percent / dimethylformamide / 24 h / 25 °C
With
chromium(VI) oxide; carbon tetrabromide; Celite; sulfuric acid; iodine; ozone; magnesium; triphenylphosphine;
In
methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetone; xylene;
5.1: Jones oxidation;
DOI:10.1246/bcsj.75.1927
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88 percent / CBr4; PPh3 / CH2Cl2 / 20 h / 0 °C
2: 97 percent / Celite; CrO3; sulfuric acid / acetone; H2O / 1 h / 0 °C
3: 85 percent / dimethylformamide / 24 h / 25 °C
With
chromium(VI) oxide; carbon tetrabromide; Celite; sulfuric acid; triphenylphosphine;
In
dichloromethane; water; N,N-dimethyl-formamide; acetone;
2: Jones oxidation;
DOI:10.1246/bcsj.75.1927
