Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

Base Information

Chemical Name:Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester
CAS No.:147510-56-3
Molecular Formula:C₂₃H₁₉ClO₆S
Molecular Weight:458.919
Hs Code.:

Synonyms:Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

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Chemical Property of Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

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Technology Process of Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

There total 3 articles about Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115481-75-9
pyridinium 2-benzenesulfonate

: 147510-56-3
Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

Guidance literature:: With phosphorus pentachloride; at 60 - 65 ℃; for 3h; under 0.1 Torr;
DOI:10.1021/jm00118a020

Reference yield:

: 34487-61-1
phenolsulphophthaleine sodium salt

: 147510-56-3
Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaBH₄, 2.) 5percent HCl / aq. ethanol / 48 h / 25 °C

2: 72 percent / 1.) RT, 4h, 2.) CH₂Cl₂, 1 h

3: PCl₅ / 3 h / 60 - 65 °C / 0.1 Torr

With hydrogenchloride; sodium tetrahydroborate; phosphorus pentachloride; In ethanol;
DOI:10.1021/jm00118a020

Reference yield:

: 172464-36-7
2-(4,4'-dihydroxy-benzhydryl)-benzenesulfonic acid

: 147510-56-3
Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1.) RT, 4h, 2.) CH₂Cl₂, 1 h

2: PCl₅ / 3 h / 60 - 65 °C / 0.1 Torr

With phosphorus pentachloride;
DOI:10.1021/jm00118a020