C₂₂H₃₄O₄

Base Information

Chemical Name:C₂₂H₃₄O₄
CAS No.:1380242-06-7
Molecular Formula:C₂₂H₃₄O₄
Molecular Weight:362.51
Hs Code.:

C<sub>22</sub>H<sub>34</sub>O<sub>4</sub>

Synonyms:C₂₂H₃₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₄O₄

Chemical Property:

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Technology Process of C₂₂H₃₄O₄

There total 9 articles about C₂₂H₃₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1380242-30-7
C₂₈H₄₈O₄Si

: 1380242-06-7
C₂₂H₃₄O₄

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 80 ℃; for 4h;
DOI:10.1002/anie.201201395

Reference yield:

: 1380242-19-2
C₂₅H₄₄O₄Si

: 1380242-06-7
C₂₂H₃₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / acetone / 16 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 80 °C

With tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran; acetone;
DOI:10.1002/anie.201201395

Reference yield:

: 1380242-15-8
C₂₅H₃₁NO₄S

: 1380242-06-7
C₂₂H₃₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

2.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 3 h / -78 °C / Inert atmosphere

3.1: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / -78 °C / Inert atmosphere

4.1: trimethylaluminum / dichloromethane; toluene / 0.5 h / -10 - 20 °C / Inert atmosphere

4.2: 8 h / -10 °C / Inert atmosphere

5.1: methyllithium / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 °C / Inert atmosphere

6.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 17 h / -30 - -15 °C / Inert atmosphere

7.1: toluene-4-sulfonic acid / acetone / 16 h / 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 80 °C

With 2,6-dimethylpyridine; tetramethylammonium triacetoxyborohydride; tetrabutyl ammonium fluoride; methyllithium; trimethylaluminum; titanium tetrachloride; diisobutylaluminium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane; acetone; toluene; acetonitrile;
DOI:10.1002/anie.201201395