3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylthioethyl)phthalamide

Base Information

• Chemical Name: 3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylthioethyl)phthalamide
• CAS No.: 942061-45-2
• Molecular Formula: C₂₄H₂₂F₇IN₆O₂S
• Molecular Weight: 718.437

Synonyms:3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylthioethyl)phthalamide

Chemical Property of 3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylthioethyl)phthalamide

Chemical Property:

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Technology Process of 3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylthioethyl)phthalamide

There total 5 articles about 3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylthioethyl)phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

3-(1,1-dimethyl-2-methylthioethylimino)-4-iodo-3H-isobenzofuran-1-one + 4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methyl aniline (942062-11-5) → 3-iodo-N1-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N2-(1,1-dimethyl-2-methylthioethyl)phthalamide (942061-45-2)

Guidance literature:

With trifluoroacetic acid; In acetonitrile; at 20 ℃; for 12h;

Reference yield:

4-n-heptafluoropropylcarbonylamino-2-methylnitrobenzene (942062-07-9) → 3-iodo-N1-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N2-(1,1-dimethyl-2-methylthioethyl)phthalamide (942061-45-2)

Guidance literature:

Multi-step reaction with 4 steps

1: carbon tetrabromide; triphenylphosphine / acetonitrile / 3 h / Heating / reflux

2: sodium azide / N,N-dimethyl-formamide / 5 h

3: hydrogen / 5%-palladium/activated carbon / ethanol / 2280.15 Torr

4: trifluoroacetic acid / acetonitrile / 12 h / 20 °C

With sodium azide; carbon tetrabromide; hydrogen; triphenylphosphine; trifluoroacetic acid; 5%-palladium/activated carbon; In ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylnitrobenzene (942062-09-1) → 3-iodo-N1-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N2-(1,1-dimethyl-2-methylthioethyl)phthalamide (942061-45-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / 5%-palladium/activated carbon / ethanol / 2280.15 Torr

2: trifluoroacetic acid / acetonitrile / 12 h / 20 °C

With hydrogen; trifluoroacetic acid; 5%-palladium/activated carbon; In ethanol; acetonitrile;

upstream raw materials:

4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methyl aniline

4-n-heptafluoropropylcarbonylamino-2-methylnitrobenzene

4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylnitrobenzene

4-nitro-3-methylaniline

Downstream raw materials:

3-iodo-N₁-[4-(5-n-heptafluoropropyltetrazol-1-yl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfonylethyl)phthalamide

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