methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate

Base Information

Chemical Name:methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate
CAS No.:1289557-79-4
Molecular Formula:C₂₂H₂₅N₃O₁₀
Molecular Weight:491.455
Hs Code.:

Synonyms:methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate

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Chemical Property of methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate

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Technology Process of methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate

There total 1 articles about methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: methyl 1,2-di-O-acetyl-3-O-benzyl-5-deoxy-5-(methoxycarbonylamino)-D-gluco-hexofuranuronate

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 1289557-79-4
methyl 2'-O-acetyl-3'-O-benzyl-1',5'-dideoxy-1'-[3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]-5'-(methoxycarbonylamino)-β-D-gluco-hexofuranuronate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 3h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2011.02.004