tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

Base Information

Chemical Name:tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane
CAS No.:351536-26-0
Molecular Formula:C₁₇H₂₂Cl₃F₃OSi
Molecular Weight:433.801
Hs Code.:

<i>tert</i>-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

Synonyms:tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

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Chemical Property of tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

Chemical Property:

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Technology Process of tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

There total 4 articles about tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 779-89-5,67801-07-4
3-(trifluoromethyl)cinnamic acid

: 351536-26-0
tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / acetone / Heating

2: DIBAL / 1 h / 0 °C

3: PDC / dimethylformamide / 1.5 h / 20 °C

4: CCl₃CO₂H / dimethylformamide / 20 °C

5: imidazole / dimethylformamide / 20 °C

With 1H-imidazole; dipyridinium dichromate; diisobutylaluminium hydride; potassium carbonate; trichloroacetic acid; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo010068c

Reference yield:

: 113048-69-4
(E)-3-(3-trifluoromethylphenyl)prop-2-en-1-ol

: 351536-26-0
tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

Guidance literature:: Multi-step reaction with 3 steps

1: PDC / dimethylformamide / 1.5 h / 20 °C

2: CCl₃CO₂H / dimethylformamide / 20 °C

3: imidazole / dimethylformamide / 20 °C

With 1H-imidazole; dipyridinium dichromate; trichloroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo010068c

Reference yield:

: 262268-58-6,871543-59-8
(E)-3-(3-(trifluoromethyl)phenyl)acrylaldehyde

: 351536-26-0
tert-butyl-dimethyl-[1-trichloromethyl-3-(3-trifluoromethyl-phenyl)-allyloxy]-silane

Guidance literature:: Multi-step reaction with 2 steps

1: CCl₃CO₂H / dimethylformamide / 20 °C

2: imidazole / dimethylformamide / 20 °C

With 1H-imidazole; trichloroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo010068c