trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

Base Information

Chemical Name:trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate
CAS No.:769968-34-5
Molecular Formula:CF₃O₃S*C₅₆H₅₁N₄P₂Pd
Molecular Weight:1097.49
Hs Code.:

trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh<sub>3</sub>)2]triflate

Synonyms:trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

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Chemical Property of trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

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Technology Process of trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

There total 3 articles about trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 769968-32-3
[Pd(3-tert-butyl-2-[(4-methylphenyl)imino]-2,3-dihydroquinazolin-4-yl)I((t)BuNC)(PPh₃)]

: 603-35-0
triphenylphosphine

: 73491-36-8
thallium(I) triflate

: 769968-34-5
trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

Guidance literature:: With H₂O; In acetone; byproducts: TlI, (CH3)3COH; addn. of phosphine and thallium salt to a soln. of palladium complex in acetone, stirring for 30 min; evapn., addn. of CH2Cl2, filtration through Celite, evapn., trituration with Et2O, filtration, washing with Et2O, drying, recrystn. (CH2Cl2/n-pentane; elem. anal.;
DOI:10.1021/om049580p

Reference yield:

: 769968-23-2
N-((2-iodophenylimino)methylene)-4-methylbenzenamine

: 769968-34-5
trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: dichloromethane

3: H₂O / acetone

With H₂O; In dichloromethane; acetone; toluene;
DOI:10.1021/om049580p

Reference yield:

: 769968-24-3
trans-[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(PPh₃)2]

: 769968-34-5
trans-[Pd(2-[(4-methylphenyl)amino]quinazolin-4-yl)(CN(t)Bu)(PPh₃)2]triflate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: H₂O / acetone

With H₂O; In dichloromethane; acetone;
DOI:10.1021/om049580p