C₃₆H₅₆O₇Si

Base Information

Chemical Name:C₃₆H₅₆O₇Si
CAS No.:350583-39-0
Molecular Formula:C₃₆H₅₆O₇Si
Molecular Weight:628.922
Hs Code.:

C<sub>36</sub>H<sub>56</sub>O<sub>7</sub>Si

Synonyms:C₃₆H₅₆O₇Si

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Chemical Property of C₃₆H₅₆O₇Si

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Technology Process of C₃₆H₅₆O₇Si

There total 11 articles about C₃₆H₅₆O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 350583-38-9
C₃₆H₅₆O₆Si

: 350583-39-0
C₃₆H₅₆O₇Si

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; In toluene; at 50 ℃; for 72h;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: C₃₉H₄₄O₇

: 350583-39-0
C₃₆H₅₆O₇Si

Guidance literature:: Multi-step reaction with 10 steps

1: 76 percent / aq. NaOH / tetrahydrofuran / 48 h / Heating

2: 93 percent / pyridine / 96 h / 20 °C

3: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

4: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

5: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

6: 99 percent / sodium periodate / tetrahydrofuran; H₂O / 72 h / 20 °C

7: 92 percent / imidazole / dimethylformamide / 5 h / 20 °C

8: 88 percent / NaBH₄ / methanol / 0.33 h / 0 °C

9: 57 percent / n-butyllithium / tetrahydrofuran; hexane / 20 h / 20 °C

10: 48 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 72 h / 50 °C

With 1H-imidazole; tert.-butylhydroperoxide; sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; formic acid; tributylphosphine; palladium diacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: 350583-27-6
1,2-benzylidene-9,10-isopropylidene-5α-acetyltaxicin-I

: 350583-39-0
C₃₆H₅₆O₇Si

Guidance literature:: Multi-step reaction with 8 steps

1: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

2: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

3: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

4: 99 percent / sodium periodate / tetrahydrofuran; H₂O / 72 h / 20 °C

5: 92 percent / imidazole / dimethylformamide / 5 h / 20 °C

6: 88 percent / NaBH₄ / methanol / 0.33 h / 0 °C

7: 57 percent / n-butyllithium / tetrahydrofuran; hexane / 20 h / 20 °C

8: 48 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 72 h / 50 °C

With 1H-imidazole; tert.-butylhydroperoxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; formic acid; tributylphosphine; palladium diacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O