3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

Base Information

Chemical Name:3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid
CAS No.:526221-11-4
Molecular Formula:C₆₇H₉₈O₁₀
Molecular Weight:1063.51
Hs Code.:

Synonyms:3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

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Chemical Property of 3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

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Technology Process of 3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

There total 8 articles about 3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 526221-10-3
C₇₁H₁₀₂O₁₁

: 526221-11-4
3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

Guidance literature:: With pyridine; water; at 130 ℃; for 2h;
DOI:10.1002/chem.200390114

Reference yield:

: 99-24-1
methyl galloate

: 526221-11-4
3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 57 percent / Amberline-120 resin / 18 h / 130 °C

2: 72 percent / K₂CO₃ / dimethylformamide / 70 °C

3: 91 percent / silica gel / methanol / 20 h / Heating

4: 79 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

5: 91 percent / aq. KOH / ethanol / 2 h / Heating

6: Et₃N / CH₂Cl₂ / 20 °C

7: 2.56 g / pyridine; H₂O / 2 h / 130 °C

With pyridine; potassium hydroxide; Amberline-120 resin; water; silica gel; potassium carbonate; triethylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200390114

Reference yield:

: 118468-30-7
4-dodecyloxybenzyl chloride

: 526221-11-4
3,4-bis(4'-dodecyloxybenzyloxy)-5-[4'-(11'-methacryloxyundecyloxy)benzyloxy]benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

2: 91 percent / aq. KOH / ethanol / 2 h / Heating

3: Et₃N / CH₂Cl₂ / 20 °C

4: 2.56 g / pyridine; H₂O / 2 h / 130 °C

With pyridine; potassium hydroxide; water; potassium carbonate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200390114