N-(4-tert-butoxybenzyl)-N₅-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N₂-(diphenylacetyl)-D-ornithinamide

Base Information

• Chemical Name: N-(4-tert-butoxybenzyl)-N₅-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N₂-(diphenylacetyl)-D-ornithinamide
• CAS No.: 1094376-15-4
• Molecular Formula: C₄₈H₅₈N₈O₆
• Molecular Weight: 843.039

Synonyms:N-(4-tert-butoxybenzyl)-N₅-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N₂-(diphenylacetyl)-D-ornithinamide

Chemical Property of N-(4-tert-butoxybenzyl)-N₅-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N₂-(diphenylacetyl)-D-ornithinamide

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Technology Process of N-(4-tert-butoxybenzyl)-N₅-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N₂-(diphenylacetyl)-D-ornithinamide

There total 1 articles about N-(4-tert-butoxybenzyl)-N₅-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N₂-(diphenylacetyl)-D-ornithinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

tert-butyl ((1Z)-(methylthio){[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methylene)carbamate (1094376-13-2) + (R)-N'-(4-tert-butoxybenzyl)-Nα-(2,2-diphenylacetyl)ornithinamide (1093677-53-2) → N-(4-tert-butoxybenzyl)-N5-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N2-(diphenylacetyl)-D-ornithinamide (1094376-15-4)

Guidance literature:

With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2008.09.033

Reference yield: 100.0%

N-(4-tert-butoxybenzyl)-N5-((E)-[(tert-butoxycarbonyl)imino]{[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methyl)-N2-(diphenylacetyl)-D-ornithinamide (1094376-15-4) + trifluoroacetic acid (76-05-1) → CHF3O3S*C39H42N8O4

Guidance literature:

In dichloromethane; for 2h;

DOI:10.1016/j.bmc.2008.09.033

upstream raw materials:

tert-butyl ((1Z)-(methylthio){[4-(4-phenyl-1H-1,2,3-triazol-1-yl)butanoyl]amino}methylene)carbamate

(R)-N'-(4-tert-butoxybenzyl)-N^α-(2,2-diphenylacetyl)ornithinamide

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