methyl 12-benzyloxy-6-oxododecanoate

Base Information

• Chemical Name: methyl 12-benzyloxy-6-oxododecanoate
• CAS No.: 1156487-94-3
• Molecular Formula: C₂₀H₃₀O₄
• Molecular Weight: 334.456
• Mol file: 1156487-94-3.mol

Synonyms:methyl 12-benzyloxy-6-oxododecanoate

Chemical Property of methyl 12-benzyloxy-6-oxododecanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of methyl 12-benzyloxy-6-oxododecanoate

There total 1 articles about methyl 12-benzyloxy-6-oxododecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl adipoyl chloride (35444-44-1) + (6-(benzyloxy)hexyl)magnesium bromide (112026-22-9) → methyl 12-benzyloxy-6-oxododecanoate (1156487-94-3)

Guidance literature:

(6-(benzyloxy)hexyl)magnesium bromide; With iron(III)-acetylacetonate; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;

methyl adipoyl chloride; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;

DOI:10.1002/chem.200801548

Reference yield: 90.0%

methyl 12-benzyloxy-6-oxododecanoate (1156487-94-3) + benzylamine (100-46-9) → methyl 6-benzylamino-12-benzyloxydodecanoate (1156488-07-1)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.200801548

upstream raw materials:

methyl adipoyl chloride

(6-(benzyloxy)hexyl)magnesium bromide

Downstream raw materials:

methyl 6-benzylamino-12-benzyloxydodecanoate