Z-PHE-LYS-2,4,6-TRIMETHYLBENZOYLOXY-METHYLKETONE TFA

Base Information

• Chemical Name: Z-PHE-LYS-2,4,6-TRIMETHYLBENZOYLOXY-METHYLKETONE TFA
• CAS No.: 118237-69-7
• Molecular Formula: C₃₄H₄₁N₃O₆*ClH
• Molecular Weight: 624.177
• Mol file: 118237-69-7.mol

Synonyms:Z-PHE-LYS-2,4,6-TRIMETHYLBENZOYLOXY-METHYLKETONE TFA;Z-Phe-Lys-2,4,6-trimethylbenzoyloxy-methylketone

Chemical Property of Z-PHE-LYS-2,4,6-TRIMETHYLBENZOYLOXY-METHYLKETONE TFA

Chemical Property:

• PSA: 174.12000
• LogP: 6.60460

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Z-PHE-LYS-2,4,6-TRIMETHYLBENZOYLOXY-METHYLKETONE TFA

There total 2 articles about Z-PHE-LYS-2,4,6-TRIMETHYLBENZOYLOXY-METHYLKETONE TFA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(S)-3-((S)-2-(((benzyloxy)carbonyl)amino)-3-phenylpropanamido)-7-((tert-butoxycarbonyl)amino)-2-oxoheptyl 2,4,6-trimethylbenzoate → N-(benzyloxycarbonyl)-L-phenylalanyl-L-lysyl <(2,4,6-trimethylbenzoyl)oxy>methyl ketone hydrochloride salt (118237-69-7)

Guidance literature:

With hydrogenchloride; In dichloromethane; 1.) 0 deg C, 15 min, 2.) RT, 2 h;

DOI:10.1021/jm00038a012

Reference yield:

N-(benzyloxycarbonyl)-L-phenylalanyl-Nε-(trifluoroacetyl)-L-lysyl <(2,4,6-trimethylbenzoyl)oxy>methyl ketone → N-(benzyloxycarbonyl)-L-phenylalanyl-L-lysyl <(2,4,6-trimethylbenzoyl)oxy>methyl ketone hydrochloride salt (118237-69-7)

Guidance literature:

With hydrogenchloride; In methanol; Ambient temperature;

DOI:10.1021/jm00038a012

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