<3R-<1(S),3R(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

Base Information

Chemical Name:<3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine
CAS No.:143444-94-4
Molecular Formula:C₁₅H₂₄N₂
Molecular Weight:232.369
Hs Code.:

Synonyms:<3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

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Chemical Property of <3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

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Technology Process of <3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

There total 4 articles about <3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 143444-91-1
1,1-dimethylethyl <3R-<1(S*),3R*(S*)>>-<1-<5-oxo-1-(1-phenylethyl)-3-pyrrolidinyl>ethyl>carbamate

: 143444-94-4
<3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 24h; Heating;
DOI:10.1002/jhet.5570290620

Reference yield:

: -4-<1-(hydroxyimino)ethyl>-1-(1-phenylethyl)-2-pyrrolidinone

: 143444-94-4
<3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / NH₃, H₂ / Raney nickel / methanol / 23 h / 2585.7 - 2637.5 Torr

2: 88 percent / triethylamine / CH₂Cl₂ / 20 h / Ambient temperature

3: 94 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating

With lithium aluminium tetrahydride; ammonia; hydrogen; triethylamine; nickel; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/jhet.5570290620

Reference yield:

: 143444-74-0
<4R-<1(S*),4R*(S*)>>-4-(1-aminoethyl)-1-(1-phenylethyl)-2-pyrrolidinone

: 143444-94-4
<3R-<1(S*),3R*(S*)>>-N,α-dimethyl-1-(1-phenylethyl)-3-pyrrolidinemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / triethylamine / CH₂Cl₂ / 20 h / Ambient temperature

2: 94 percent / lithium aluminium hydride / tetrahydrofuran / 24 h / Heating

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jhet.5570290620