(E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

Base Information

Chemical Name:(E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate
CAS No.:139305-48-9
Molecular Formula:2C₂H₂O₄*C₂₈H₃₀N₂O
Molecular Weight:590.63
Hs Code.:

(E)-1-(3-Methyl-6,11-dihydrodibenz<b,e>oxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

Synonyms:(E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

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Chemical Property of (E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

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Technology Process of (E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

There total 6 articles about (E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 18903-01-0,114312-65-1,87179-40-6
trans-1-cinnamylpiperazine

: 87673-23-2
11-Chloro-3-methyl-6,11-dihydro-dibenzo[b,e]oxepine

: 139305-48-9
(E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

Guidance literature:: In dichloromethane; for 1h; Ambient temperature;
DOI:10.1248/cpb.39.2564

Reference yield:

: 87-41-2
2-benzofuran-1(3H)-one

: 139305-48-9
(E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

Guidance literature:: Multi-step reaction with 5 steps

1: 1 h / 200 °C

2: 89 percent / (CF₃CO)2O, BF₃*Et₂O / CH₂Cl₂ / 1 h / Ambient temperature

3: NaBH₄ / methanol / 0.33 h / 0 °C

4: SOCl₂ / 0.17 h / Ambient temperature

5: 48 percent / CH₂Cl₂ / 1 h / Ambient temperature

With sodium tetrahydroborate; thionyl chloride; boron trifluoride diethyl etherate; trifluoroacetic anhydride; In methanol; dichloromethane;
DOI:10.1248/cpb.39.2564

Reference yield:

: 23560-72-7
3-Methyl-6,11-dihydrodibenzoxepin-11-one

: 139305-48-9
(E)-1-(3-Methyl-6,11-dihydrodibenzoxepin-11-yl)-4-(3-phenyl-2-propenyl)piperazine dioxalate

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / 0.33 h / 0 °C

2: SOCl₂ / 0.17 h / Ambient temperature

3: 48 percent / CH₂Cl₂ / 1 h / Ambient temperature

With sodium tetrahydroborate; thionyl chloride; In methanol; dichloromethane;
DOI:10.1248/cpb.39.2564