ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

Base Information

Chemical Name:ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate
CAS No.:107408-25-3
Molecular Formula:C₃₀H₃₀IO₃P
Molecular Weight:596.445
Hs Code.:

Synonyms:ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

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Chemical Property of ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

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Technology Process of ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

There total 4 articles about ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107408-20-8
5,5-dimethoxy-1-iodo-1(Z)-pentene

: 107408-25-3
ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / 50percent aq. HOAc / 14 h

2: 91 percent / tetrahydrofuran; diethyl ether / 15 h / 0 °C

3: 56 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h

4: NaH, 2-propanol / 1.5 h

With sodium hydride; acetic acid; isopropyl alcohol; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 107408-23-1
6-iodo-5(Z)-hexen-2-ol

: 107408-25-3
ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h

2: NaH, 2-propanol / 1.5 h

With sodium hydride; isopropyl alcohol; pyridinium chlorochromate; In dichloromethane;

Reference yield:

: 107408-21-9
(Z)-5-iodo-4-pentenal

: 107408-25-3
ethyl 9-iodo-5-methyl-3-oxo-2-(triphenylphosphoranylidene)-4(E),8(Z)-nonadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / tetrahydrofuran; diethyl ether / 15 h / 0 °C

2: 56 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h

3: NaH, 2-propanol / 1.5 h

With sodium hydride; isopropyl alcohol; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;