(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

Base Information

Chemical Name:(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride
CAS No.:1447760-49-7
Molecular Formula:C₂₃H₂₃N₃O₁₅*ClH
Molecular Weight:617.908
Hs Code.:

Synonyms:(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

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Chemical Property of (2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

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Technology Process of (2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

There total 6 articles about (2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1447760-37-3
(2-acetyloxybenzoyl)oxymethyl 3-[3-(tert-butoxycarbonylamino)propanoyloxy]-4-(2,3-bisnitrooxypropoxy)benzoate

: 1447760-49-7
(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/cmdc.201300105

Reference yield:

: 1447760-17-9
2-(allyloxy)-5-formylphenyl 3-[(tert-butoxycarbonyl)amino]propanoate

: 1447760-49-7
(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: silver nitrate; iodine / acetonitrile / 17 h / -15 - 70 °C

2: potassium permanganate / acetone / 1 h / 0 - 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

4: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; potassium permanganate; iodine; caesium carbonate; silver nitrate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/cmdc.201300105

Reference yield:

: 79822-65-4
3-hydroxy-4-(2-propenyloxy)benzaldehyde

: 1447760-49-7
(2-acetyloxybenzoyl)oxymethyl 3-(3-aminopropanoyloxy)-4-(2,3-bisnitrooxypropoxy)benzoate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: silver nitrate; iodine / acetonitrile / 17 h / -15 - 70 °C

3.1: potassium permanganate / acetone / 1 h / 0 - 20 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; potassium permanganate; iodine; caesium carbonate; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/cmdc.201300105