benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine

Base Information

• Chemical Name: benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine
• CAS No.: 633296-91-0
• Molecular Formula: C₂₈H₄₆N₂O₂
• Molecular Weight: 442.685

Synonyms:benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine

Chemical Property of benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine

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Technology Process of benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine

There total 1 articles about benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

Methanesulfonate3-[3-[(E)-benzylimino]-1-(5,5-dimethyl-[1,3]dioxan-2-ylmethyl)-propyl]-1-butyl-5-ethyl-pyridinium; → benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine (633296-91-0) + benzyl-[3-(1-butyl-5-ethyl-1,2,5,6-tetrahydro-pyridin-3-yl)-4-(5,5-dimethyl-[1,3]dioxan-2-yl)-butyl]-amine

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃;

DOI:10.1021/jo034099e

Reference yield: 70.0%

benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine (633296-91-0) → 1-benzyl-1'-butyl-5'-ethyl-1,2,3,6,1',2',3'4'5'6'-decahydro[3',4]bipyridinyl

Guidance literature:

benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine; With hydrogenchloride; In 1,4-dioxane; at 50 ℃;

With sodium tetrahydroborate; In 1,4-dioxane; at 20 ℃; for 5h;

DOI:10.1021/jo034099e

Reference yield: 45.0%

benzyl[3-(1-butyl-5-ethyl-1,2,3,6-tetrahydro-pyridin-3-yl)4-(5,5-dimethyl[1,3]dioxan-2-yl)-butyl]amine (633296-91-0) → 1-(1-benzyl-1'-butyl-5'-ethyl-1,2,3,6,1',2',3'4'5'6'-decahydro[3',4]bipyridin-2-yl)propan-2-one

Guidance literature:

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In water; acetone; for 30h; Heating;

DOI:10.1021/jo034099e

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