((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

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Chemical Name:((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester
CAS No.:760979-74-6
Molecular Formula:C₂₉H₃₀N₄O₁₄
Molecular Weight:658.576
Hs Code.:

((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

Synonyms:((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

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Chemical Property of ((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

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Technology Process of ((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

There total 12 articles about ((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 540496-34-2
(S)-(2-oxo)oxazolidine-4-acetic acid benzyl ester

: 760979-73-5
[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetic acid pentafluorophenyl ester

: 760979-74-6
((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1039/b405856a

Reference yield:

: 87219-29-2
benzyl (3S)-5-oxotetrahydro-3-furanylcarbamate

: 760979-74-6
((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 11 steps

1.1: aq. Cs₂CO₃ / acetone / 3 h / Heating

1.2: 60 percent / dimethylformamide / 24 h / 20 °C

2.1: 95 percent / DIEA; DMAP / dimethylformamide / 24 h / 20 °C

3.1: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

4.1: 100 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

5.1: 70 percent / DIEA; DMAP / dimethylformamide / 16 h / 20 °C

6.1: 92 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

7.1: 95 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

8.1: 50 percent / DIEA; DMAP / dimethylformamide / 16 h / 20 °C

9.1: 92 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

10.1: 95 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

11.1: 50 percent / DIEA; DMAP / dimethylformamide / 16 h / 20 °C

With pyridine; dmap; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1039/b405856a

Reference yield:

: 1152-61-0
N-Cbz-L-Asp

: 760979-74-6
((S)-3-{2-[(S)-3-(2-{(S)-3-[2-((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetyl]-2-oxo-oxazolidin-4-yl}-acetyl)-2-oxo-oxazolidin-4-yl]-acetyl}-2-oxo-oxazolidin-4-yl)-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 13 steps

1.1: 95 percent / Ac₂O / 0.02 h / microwave irradiation

2.1: 80 percent / NaBH₄ / tetrahydrofuran / 16 h / 20 °C

3.1: aq. Cs₂CO₃ / acetone / 3 h / Heating

3.2: 60 percent / dimethylformamide / 24 h / 20 °C

4.1: 95 percent / DIEA; DMAP / dimethylformamide / 24 h / 20 °C

5.1: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

6.1: 100 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

7.1: 70 percent / DIEA; DMAP / dimethylformamide / 16 h / 20 °C

8.1: 92 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

9.1: 95 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

10.1: 50 percent / DIEA; DMAP / dimethylformamide / 16 h / 20 °C

11.1: 92 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

12.1: 95 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

13.1: 50 percent / DIEA; DMAP / dimethylformamide / 16 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; hydrogen; acetic anhydride; caesium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1039/b405856a