2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose
CAS No.:898224-25-4
Molecular Formula:C₅₅H₅₂O₁₄
Molecular Weight:937.009
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

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Chemical Property of 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

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Technology Process of 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

There total 1 articles about 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 53270-12-5
1,2-O-(1-ethoxyethylene) 3,4,6-tri-O-benzyl-1-thio-α-D-glucopyranose

: 502765-04-0
2,3,4-tri-O-benzoyl-α,β-D-xylopyranosyl trichloroacetimidate

: 898224-25-4
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

Guidance literature:: 1,2-O-(1-ethoxyethylene) 3,4,6-tri-O-benzyl-1-thio-α-D-glucopyranose; With sulfuric acid; In ethanol; ethyl acetate; at 20 ℃;

2,3,4-tri-O-benzoyl-α,β-D-xylopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -20 ℃;
DOI:10.1016/j.carres.2006.02.036

Reference yield:

: 898224-25-4
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

: C₅₃H₄₉BrO₁₂

Guidance literature:: With hydrogen bromide; In dichloromethane; acetic acid; at 20 ℃; for 6h;
DOI:10.1016/j.carres.2006.02.036

Reference yield:

: 898224-25-4
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-1-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranose

: 898224-27-6
7-O-benzyl-3-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->2)-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-tamarixetin

Guidance literature:: Multi-step reaction with 2 steps

1: 118 mg / HBr / acetic acid; CH₂Cl₂ / 6 h / 20 °C

2: 68 mg / Bu₄NBr; K₂CO₃ / CHCl₃; H₂O / 20 h / 50 °C

With tetrabutylammomium bromide; hydrogen bromide; potassium carbonate; In dichloromethane; chloroform; water; acetic acid;
DOI:10.1016/j.carres.2006.02.036